| Week | Lecture # | Week of... | Topic(s) | Chapter(s) |
| 1 | Lecture 1 Lecture 2 | August 26th | Concepts, data analysis | 1 |
| 2 | Lecture 3 Lecture 4 Lecture 5 | August 31st | Sample prep, solution chemistry | 1 |
| 3 | Lecture 6 Lecture 7 | September 9th | Light-matter interaction, optics | 2 |
| 4 | Lecture 8 Lecture 9 Lecture 10 | September 14th | NMR | 3 |
| 5 | Lecture 11 Lecture 12 | September 21st | 2-D NMR, solid state NMR | 3 |
| 6 | Lecture 13 Lecture 14 Exam 1 | September 28th | IR spectroscopy | 4 |
| 7 | Lecture 15 Lecture 16 Lecture 17 | October 5th | IR spectroscopy | 4 |
| 8 | Lecture 18 Lecture 19 Lecture 20 | October 12th | UV-Vis, Fluorescence | 5 |
| 9 | Lecture 21 Lecture 22 Lecture 23 | October 19th | Atomic absorption | 6 |
| 10 | Lecture 24 Lecture 25 Lecture 26 | October 26th | Atomic emission | 7 |
| 11 | Lecture 27 Lecture 28 Exam 2 | November 2nd | Mass Spectrometry | 9, 10 |
| 12 | Lecture 29 Lecture 30 | November 9th | Gas Chromatography | 12 |
| 13 | Lecture 31 Lecture 32 Lecture 33 | November 16th | Liquid Chromatography | 13 |
| 14 | Lecture 34 Lecture 35 | November 23rd | Electrophoresis | 13 |
| 15 | Lecture 36 Lecture 37 Lecture 38 | November 30th | X-ray techniques | 8 |
| 16 | Lecture 39 Exam 3 | December 7th | X-ray techniques | 8 |